The power of electrochemical measurements in respect of thermodynamics,
kinetics and analysis is widely recognised but the subject can be
unpredictable to the novice even if they have a strong physical and
chemical background, especially if they wish to pursue quantitative
measurements. Accordingly, some significant experiments are perhaps
wisely never attempted while the literature is sadly replete with flawed
attempts at rigorous voltammetry.This textbook considers how to
implement designing, explaining and interpreting experiments centered on
various forms of voltammetry (cyclic, microelectrode, hydrodynamic,
etc.). The reader is assumed to have knowledge of physical chemistry
equivalent to Master's level but no exposure to electrochemistry in
general, or voltammetry in particular. While the book is designed to
stand alone, references to important research papers are given to
provide an introductory entry into the literature.The third edition
contains new material relating to electron transfer theory, experimental
requirements, scanning electrochemical microscopy, adsorption,
electroanalysis and nanoelectrochemistry.