Chapter-I presents a brief summary of the various thin film deposition
techniques, their merits and demerits. The various reports on the
electrodeposition of elemental, binary and ternary semiconductors have
also been surveyed in this chapter. A review of the basic principles
involved in the electrodeposition of the semiconductors is also given
Chapter-II and III deal with the development of electrodeposition
technique for CuInSe2 films.An alternative route to fabricate CuInSe2
films are explored. This consisted of electroplating a binary system
comprising of Cu and In and vacuum evaporating thick selenium film over
it for further selenisation treatment. Electrodeposition characteristics
of Cu, In and Cu-In in the nonaqueous bath employing ethylene glycol as
the solvent are discussed in chapter II. The compositional, structural
and morphological analysis of the electrodeposits was also performed and
the results have been presented in this chapter. Chapter III deals with
the development of rapid thermal annealing technique for the preparation
of CuInSe2 films from the Cu-In/Se layers